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Synthesis and characterization of SO42-/KCC-1 catalyst as an alternative candidate for simultaneous esterification and transesterification reactions

Journal Of Natural Sciences And Mathematics Research

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Title Synthesis and characterization of SO42-/KCC-1 catalyst as an alternative candidate for simultaneous esterification and transesterification reactions
 
Creator Farikhah, Ginda Putri
Udaibah, Wirda
Mulyatun, Mulyatun
 
Subject applied sciences
KCC-1; SO42-/KCC-1; impregnation; esterification; transesterification
 
Description Sulfate-impregnated acid catalysts can be used to replace conventional homogeneous base catalysts which are very dangerous, corrosive and environmentally unfriendly. Sulfate impregnation on porous support material will increase the surface area of the catalyst. The use of KCC-1 as a supporting material can produce catalysts with excellent properties. The method used in this research is the hydrothermal method for the synthesis of KCC-1 and the direct impregnation method for the synthesis of SO42-/KCC-1. Characterization of the resulting material using X-ray diffraction (XRD), FTIR spectrometer, and low temperature emission scanning electron microscope (SEM). The characterization results showed that the synthesis of KCC-1 and SO42-/KCC-1 had been successfully carried out. This is evidenced by the formation of amorphous silica, the presence of peaks of silica and sulfate groups, and scanning electron microscope images showing nano-sized materials.©2021 JNSMR UIN Walisongo. All rights reserved. 
 
Publisher Faculty of Science and Technology, Universitas Islam Negeri Walisongo Semarang
 
Contributor —
 
Date 2022-04-06
 
Type info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
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Format application/pdf
 
Identifier https://journal.walisongo.ac.id/index.php/JNSMR/article/view/6797
10.21580/jnsmr.2021.7.1.6797
 
Source Journal Of Natural Sciences And Mathematics Research; Vol 7, No 1 (2021): Volume 7, Nomor 1, 2021; 8-13
2460-4453
2614-6487
 
Language eng
 
Relation https://journal.walisongo.ac.id/index.php/JNSMR/article/view/6797/pdf
 
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